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Test Sample Chromatograms
Test sample chromatograms
239
SAMPLE:
Type FPD Sample
Inj Volume 1
l
Part No. 19395•60580
COMPOSITION: 20 ng/
L
(20.0 ppm W/V) each of
1-dodecanethiol and
tributylphosphate in isooctane
Detector Type FPD
Temp 200 DEGREES C
Inlet Type DED ON-COL CAP
Oven Track On
Temp N/A DEGREES C
Operating Mode N/A
Purge Time On N/A min
Purge Time Off N/A
min
Oven Temp Programmed (1 ramp)
Init Temp 90
DEGREES C
Init Time 1.0
min
Ramp (1) (2)
Rate 20
10
Fin Temp 110 170
Fin Time 0 3
Flow Param (EPP)
Constant Flow Off
Range 5
COLUMN:
Part No. 19095S•100
Dimensions 5 M Length, 530 ID
Sta Phase Methyl
Silicone
1.45
4.08
4.57
5.37
START
IF
.13
.49
Phosphorus
Filter
Sulfer
Filter
IF
START
.13
1.91
4.06
3.35
HP 5890 Test Sample Operating
Conditions
DODECANETHIOL
TRIBUTYLPHOS-
PHATE
FLOW RATES (FPD AIR MODE FLOWS)
Carrier (N2) 20 +/• 1 ml/min
Hydrogen 75 +/• 2 ml/min
Air 100 +/• 3 ml/min
Makeup (N2) 0 ml/min
Split Vent N/A ml/min
Septum Purge 5 +/• 1 ml/min
FPD On-column Inlet
Figure 10-15.