Test Sample Chromatograms
Test sample chromatograms
230
Detector Type FIDw/MUG
Temp 250 DEGREES C
Inlet Type SPLIT ONLY
OR
SPLIT/SPLITLESS Temp 200
DEG C
Operating Mode SPLIT(PURGE
ON)
Purge Time On 0
min
Purge Time Off 0
min
Oven Temp Programmed (1 ramp)
Init Temp 100
DEGREES C
Init Time 0
min
Ramp
Rate 20
Fin Temp 180
Fin Time 1
Range 7
COLUMN:
Part No. 19095Z•121
Dimensions 530 ;10M
Sta Phase Methyl
Silicone
FLOW RATES
Carrier (He) 15 +/• 1 ml/min
Hydrogen 30 +/• 1 ml/min
Air 400 +/• 20 ml/min
Makeup (N2) 20 +/• 1 ml/min
Split Vent 200 +/• 20 ml/min
Septum Purge 5 +/• 1 ml/min
SAMPLE:
Type Capillary Sample
Inj Volume 1
l
Part No. 18740•60900
Composition: Soln of 0.1%(w/w)
n-nonane,n-hexadecane and 0.1%
(w/w)each of 1-octanol,nonanol,
n-undecane,naphthalene,2-deca-
none,n-dadecane,n-tridecane,
1-pentadecane in tetradecane.
.40
2.21
2.35
2.81
2.64
3.67
ST
START
C9
C16
HP 5890 Test Sample Operating Conditions
FID-Split Mode Capillary Inlet
Figure 10-6.
